FIELD: organic chemistry. SUBSTANCE: solution of organomagnesium compound of the general formula , where R′=C2H5, i=C4H9, R″=н=C4H9, i=C5H11; a = 0,01-0,1; b = 0,5-2,0, in chloro- benzene is interacted with CCl4 at mole ratio CCl4/Mg = 3-5 at 50-70 C following by treatment of solid product formed with solution of ethylaluminium chloride of the general formula (ElAlCl2,El2AlCl,El3Al2Cl3) and then - with solution of TiCl4 or VOCl3 at mole ratio Al/Mg = 0,5-2,0 and Ti(V)/Mo= 0,01-0,1 at 20-60 C. Method is used for synthesis of catalyst. EFFECT: improved method of synthesis. 1 tbl
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Authors
Dates
1994-02-15—Published
1990-04-20—Filed