6-CHLORO-5,5-DIMETHYL-4-OXA-1-HEXINE SHOWING ANTIMICROBIAL ACTIVITY IN LUBRICATING OILS Russian patent published in 1994 - IPC

Abstract RU 2015136 C1

FIELD: organic chemistry. SUBSTANCE: product: 6-chloro-5.5-dimethyl-4-oxa-1-hexine of the general formula ClCH2C(CH3)2OCH2C ≡ CH, b.p. is 66-68 C, d24

0 0,9997, n2D
0=1,4560, MRD 39,86 (calculated), and 39.08 (found), yield is 75%. Reagent 1: propargyl alcohol. Reagent 2: metallyl chloride. Reaction conditions: in the presence of para-toluenesulfoacid, in sealed ampoule. Synthesized compound shows antimicrobial activity with regard to lubricating oils. EFFECT: improved method of synthesis. 1 tbl

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RU 2 015 136 C1

Authors

Aliev S.M.

Sadykhov K.I.

Karaev S.F.

Talybov G.M.

Gadzhieva M.A.

Askerova S.A.

Dates

1994-06-30Published

1991-01-02Filed