FIELD: analytical chemistry. SUBSTANCE: method involves the steps of: treating a sample to be analyzed by a concentrated sulfuric acid containing 10% of potassium nitrate under heating conditions at 60 degrees C, diluting a reaction mixture with water, alcalizing with sodium hydroxide solution, then providing pH of medium equal to 5, treating with crystalline violet solution, extracting a reaction product with toluene and photometering the extract. EFFECT: enhanced accuracy. 1 dwg
Authors
Dates
1994-11-15—Published
1991-04-15—Filed