FIELD: organic chemistry. SUBSTANCE: product: 1-ethyl-2-methyl-1H-pyrido[3,2-k, l]phenothiazine, empirical formula is C18H17NS, m. p. is 70-71 C. Reagent 1: 1-ethyl-2-methyl-3-(10-phenothiazinyl)-2,3-dihydro-1H-pyrido[- 3,2-k, l] phenothazine. Reagent 2: acetic acid chloroanhydride. Reaction conditions: heating at the range 60-100 C. EFFECT: improved method of synthesis. 3 cl, 2 tbl
Authors
Dates
1995-03-10—Published
1991-12-24—Filed