FIELD: agriculture. SUBSTANCE: the product is trans-4-azido-3, 6- dimethylhexahydropyridin-2-thione of the formula: C6H11N5S. The yield 89.5-97.8% mp 126.5-127.5. Reagent 1: 4 hydroxy-3,6-dimethylhexahydropyridin-2-thione. Reagent 2: sodium azide. Reaction conditions: concentrated hydrochloric acid, 20 C. EFFECT: improved properties of the title compound. 3 tbl
Title | Year | Author | Number |
---|---|---|---|
BIS(OXYMETHYL)PHENYL(CARBOXYMETHYL)PHOSPHONIUM CHLORIDE HAVING NEMATOCIDE ACTIVITY | 0 |
|
SU1641826A1 |
(2-3′--NITROPHENOXY)-2-THIO-3-ISOPROPYL-1,3,2-OXAZAPHOSPHORINANE SHOWING NEMATOCIDE ACTIVITY AGAINST GALLIC NEMATODES | 1991 |
|
RU2053235C1 |
TRANS-4,5-DIAZIDOIMIDAZOLIDIN 2-ONE HAVING FUNGICIDAL ACTIVITY | 1993 |
|
RU2034838C1 |
2-ALKOXY-2-THIO-5-(N-PHENYLCARBAMOYL) | 1996 |
|
RU2105771C1 |
METHOD OF PRODUCING CIS-1-0-(1-ALKENYL)-GLYCERIN | 0 |
|
SU1293167A1 |
METHOD OF OBTAINING 3-(BETA-D-GLUCOPYRANOSYL)-4-OXYHEXAHYDROPYRIMIDINE-2-THION | 0 |
|
SU1366517A1 |
4,5-DIHYDRO-4-(O,O-DIETHYLTHIOPHOSPHORYL)-5-METHYL-1,2,4-TRIA- ZINE-6-ONE SHOWING INSECTICIDIC AND ACARICIDIC ACTIVITY | 1988 |
|
SU1527872A1 |
1-(DIETHYLTHIOPHOSPHORYLTHIO)METHYL-5-METHYL-4,5-DIHYDRO-6-OXO-1,2,4-TRIAZINES HAVING INSECTICIDE AND ACARICIDE ACTIVITIES | 1989 |
|
SU1621453A1 |
1-NAPHTHYLACETYL-1,1,1-TRITRIMETHYLHYDRAZINIUM IODIDE DISPLAYING RETARDENT ACTIVITY FOR TOMATO CULTURES | 0 |
|
SU1080411A1 |
METHOD OF OBTAINING (5,5-DICHLOR-2, 4-DIOXO-2-CYCLOPENTENONE)-PYRIDINE BETAINE | 0 |
|
SU522600A1 |
Authors
Dates
1995-07-09—Published
1993-06-30—Filed