FIELD: analytical chemistry. SUBSTANCE: method involves preliminary activation of silica gel by boiling in 15-18% hydrochloric acid solution at their volume ratio 1:2, washing out of chloride ions with water and drying firstly at 95-105 C and then at 150 C for 1 h. Then air analyzed mixture is passed and dimethylformamide is eluted with aqueous-spirituous mixture followed by alcohol evaporation. EFFECT: improved method of assay. 2 tbl
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Authors
Dates
1995-09-27—Published
1992-06-18—Filed