FIELD: organic chemistry. SUBSTANCE: 2,4-diethyloctyl acetate of formula (I) as component of perfume compositions, 2,4- diethyloctyl acetate is prepared by reacting acetic acid with 2,4-diethyloctanol under conditions of azeotropic distillation of water. The azeotropic agent is cyclohexane or mixture thereof with ethyl acetate. The catalyst is 2-hydroxy-5-sulfobenzoic acid. The structure of the compound of formula I is given in the specification. EFFECT: improved properties of the title compound. 3 cl
Title | Year | Author | Number |
---|---|---|---|
2,4-DIETHYL OCTANAL ETHYLENE GLYCOL ACETAL AS COMPONENT IN PERFUME COMPOSITIONS AND AROMAS | 1993 |
|
RU2037490C1 |
2-ACETONYL-5,5-DIMETHYL-1,2,3,4,5,6,7,8-OCTAHYDRONAPHTHALENE AS A COMPONENT OF PERFUMERY COMPOSITION, METHOD OF ITS SYNTHESIS, 2,6-DIMETHYL-2,6,10-TRIDECATRIENE-12-ONE AS AN INTERMEDIATE PRODUCT IN SYNTHESIS OF 2-ACETONYL-5,5-DIMETHYL-1,2,3,4,5,6,7,8-OCTAHYDRONAPHTHALENE | 1992 |
|
RU2035448C1 |
COMPONENT FOR PERFUME COMPOSITIONS | 1992 |
|
RU2041925C1 |
0 |
|
SU526656A1 | |
COMPOSITION OF FRAGRANT SUBSTANCE SHOWING IRIS OIL ODOR | 1993 |
|
RU2057171C1 |
PERFUME COMPOSITION | 0 |
|
SU863626A1 |
2-ACETONOYL-3,3,5,5-TETRAMETHYL-@@@9,10-OCTALINE AS A COMPONENT OF PERFUMERY COMPOSITIONS | 0 |
|
SU1578123A1 |
0 |
|
SU529167A1 | |
UNSYMMETRICAL OXALIC ACID ESTERS AS FRAGRANT SUBSTANCES WITH FLOWER-FRUIT SCENT | 0 |
|
SU1150247A1 |
AROMATIC PRINCIPLE COMPOSITION | 1995 |
|
RU2081897C1 |
Authors
Dates
1996-03-27—Published
1992-08-13—Filed