METHOD OF SYNTHESIS OF ARYLTRIAZOLINONE Russian patent published in 1998 - IPC

Abstract RU 2119918 C1

FIELD: organic chemistry and chemical technology. SUBSTANCE: invention relates to synthesis of 1-aryltriazolinone of the formula (I) where R is a lower alkyl; X is halogen, lower alkyl, nitro-, hydroxy-groups, -NHSO2R′,-N(SO2R′)2,-N(R′)SO2R′; R' is a lower alkyl; n is a whole number from 0 to 3. Method involves treatment of aryltriazolidinone of the formula (II) with hypohalogenous acid or its salt in tert.-butanol-water medium at weight ratio = (95-70): (5-30), respectively. EFFECT: improved method of synthesis, high purity degree and yield of the end product. 9 cl, 8 ex

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RU 2 119 918 C1

Authors

Allan R.Behjli

Mark Khehlfon

Ehrik Uill'Jam Sortor

Dates

1998-10-10Published

1993-04-29Filed