FIELD: organic chemistry and technology. SUBSTANCE: method of synthesis of 2-(2,6-dichloro-phenylamino)-2-imidazoline hydrochloride involves the interaction of 2,6-dichloroaniline with 1-acetyl-2-imidazo-lidone in medium of phosphorus oxychloride at 75-80 C for 7.5-8 h followed by treatment of the formed derivative of 2-imidazolidine with methanol. EFFECT: accelerated process of clophelin synthesis. 1 tbl, 12 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PRODUCING 2-(2,6-DICHLOROPHENYLAMINO)-2-IMIDAZOLINE HYDROCHLORIDE | 2017 |
|
RU2652125C1 |
METHOD OF PREPARING SUBSTITUTED 2-(PHENYLAMINO)-2- IMIDAZOLINES | 1997 |
|
RU2131872C1 |
METHOD FOR PREPARING 5-CHLORO-4-[(2-IMIDAZOLINE-2-YL)AMINO]-2,1,3-BENZOTHIADIZOLE | 2003 |
|
RU2237669C1 |
METHOD OF OPTICALLY ACTIVE IMIDAZOLIDINE-2-THIONE DERIVATIVES | 0 |
|
SU791231A3 |
0 |
|
SU548207A3 | |
0 |
|
SU509589A1 | |
0 |
|
SU511000A3 | |
PROCESS FOR PREPARING 2-SUBSTITUTED 1,4-BENZODIAZEPINES | 0 |
|
SU1126209A3 |
METHOD OF PREPARING SUBSTITUTED DIPHENYLAMINE | 1999 |
|
RU2178784C2 |
METHOD OF PRODUCING 2-BROMO-6-FLUORO-N-2-IMIDAZOLIDINYLIDENE-BENZAMINE OR ITS SALT | 0 |
|
SU665800A3 |
Authors
Dates
1999-07-20—Published
1997-02-18—Filed