FIELD: production of polymers, synthetic rubber industry, particularly, methods of production of ethylene-propylene or ethylene-propylenediene copolymer in offered mixing reactor. SUBSTANCE: method of continuous copolymerization in solution includes dissolving in hydrocarbon solvent of monomers, hydrogen and catalytic complex components; supply of solution of gas-liquid mixture containing monomers, solvent and hydrogen into lower part of reactor provided with mixer; supply of solutions of catalytic complex components into reactor; copolymerization in mixing of reaction mass at high pressure and temperature. Method is distinguished by the fact that preparation of gas-liquid mixture of monomers, hydrogen, solvent and separate dissolving of catalytic complex components in solvent are carried out in flow with turbulent mixing in tubular nozzles in respective inlet pipe unions of reactor at flow velocity of, at least, 3 ± 2 m/s for gas-liquid mixture and, at least, 0.3 m/s for components of catalytic complex. Description of reactor for embodiment of the claimed method is offered. EFFECT: efficiency method and device for continuous polymerization in solution with production of uniform copolymer. 2 cl, 4 dwg, 1 tbl
Title | Year | Author | Number |
---|---|---|---|
METHOD OF CONTINUOUS COPOLYMERIZATION IN SOLUTION AND REACTOR FOR ITS EMBODIMENT | 1998 |
|
RU2141872C1 |
METHOD OF PRODUCTION OF ETHYLENE-PROPYLENE COPOLYMERS AND POLYMERIZER FOR ITS EMBODIMENT | 1998 |
|
RU2141871C1 |
CONTINUOUS SOLUTION COPOLYMERIZATION PROCESS AND POLYMERIZER FOR CONDUCTING THE PROCESS | 2000 |
|
RU2175659C1 |
METHOD OF CONTINUOUS SOLUTION COPOLYMERIZATION AND REACTOR-DISTRIBUTOR FOR ITS EMBODIMENT | 1998 |
|
RU2144843C1 |
CONTINUOUS SOLUTION COPOLYMERIZATION PROCESS | 2001 |
|
RU2207346C2 |
METHOD OF CONTINUOUS SOLUBLE COPOLYMERIZATION AND POLYMERIZATION REACTOR FOR CARRYING IT OUT | 2000 |
|
RU2174128C1 |
CONTINUOUS SOLUTION COPOLYMERIZATION PROCESS AND POLYMERIZER FOR IMPLEMENTATION THEREOF | 2000 |
|
RU2177957C2 |
CONTINUOUS SOLUTION COPOLYMERIZATION PROCESS AND POLYMERIZER FOR IMPLEMENTATION THEREOF | 2001 |
|
RU2207345C2 |
METHOD OF CONTINUOUS SOLUBLE COPOLYMERIZATION AND POLYMERIZATION REACTOR FOR CARRYING IT OUT | 2000 |
|
RU2174521C1 |
METHOD AND DEVICE FOR CONTINUOUS SOLUTION COPOLYMERIZATION | 2000 |
|
RU2169738C1 |
Authors
Dates
1999-11-27—Published
1998-07-08—Filed