METHOD FOR OBTAINING (METH)ACRYLIC ACID Russian patent published in 2008 - IPC C07C51/215 C07C51/25 C07C51/44 C07C51/46 C07C57/07 C07C67/54 C07C69/54 B01D3/14 B01D3/36 B01D3/40 B08B9/08 B01D3/34 

Abstract RU 2333194 C2

FIELD: chemistry.

SUBSTANCE: invention concerns improved method for obtaining (meth)acrylic acid involving steam phase catalytic oxidation of propylene, propane or isobutylene for production of reaction mix, absorption of oxidised reaction product in water to obtain water solution containing (meth)acrylic acid, concentration of water solution in the presence of azeotropic agent and distillation of obtained (meth)acrylic acid in distillation column to obtaining purified (meth)acrylic acid. During operation of distillation column, including operation interruption and resumption, the column is washed with water, and afterwards azeotropic distillation is performed in the presence of azeotropic agent.

EFFECT: efficient and fast cleaning of distillation column with extraction of valuable substance.

5 cl, 5 dwg, 3 ex

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RU 2 333 194 C2

Authors

Jada Sukhei

Ogava Jasusi

Takasaki Kendzi

Suzuki Esiro

Dates

2008-09-10Published

2003-09-02Filed