FIELD: technological processes.
SUBSTANCE: invention is related to production of valve metal powders. Valve metal compounds are reduced by alkaline metal in the presence of thinner salt. Reduction is done in the presence of substance that helps to decrease granules, which is added to reaction mixture periodically or continuously. Valve metal compound used is K2TaF7, Na2TaF7 or their mixture. Substance used to assist in decrease of granules, sulfur-containing, phosphor-containing, boron-containing and/or silicon-containing compounds are used.
EFFECT: production of valve metal powders with high specific surface and uniform distribution of size.
10 ex, 11 cl
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Authors
Dates
2009-07-27—Published
2004-12-09—Filed