METHOD OF OBTAINING N-2-ETHYLHEXYL-N'-PHENYL- п -PHENYLENEDIAMINE Russian patent published in 2009 - IPC C07C211/51 C07C211/55 C07C209/16 

Abstract RU 2362767 C1

FIELD: chemistry.

SUBSTANCE: invention relates to method of obtaining N-2-ethylhexyl-N'-phenyl-п-phenylenediamine, which is used as antioxidant for polymers by alkylation of n-aminodiphenylamine with aliphatic alcohols at temperature 170-235°C in presence of potassium hydroxide with distillation of alcohol azeotrope with water through refluxer, in which s temperature 90-110°C is supported, by return of condensed hot alcohol in reaction zone, by separating of target product from organic layer after water extraction of reaction mass.

EFFECT: increasing of product quality by reduction of alkylation time.

3 cl, 4 ex, 1 tbl

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RU 2 362 767 C1

Authors

Vinokurov Jurij Valentinovich

Filippov Valerij Mikhajlovich

Kavun Semen Moiseevich

Ivanov Vladimir Aleksandrovich

Jaskova Marija Sergeevna

Dates

2009-07-27Published

2007-12-18Filed