METHOD OF MAKING SORBENT FOR SEPARATING FULLERENES Russian patent published in 2009 - IPC B01J20/283 

Abstract RU 2373992 C1

FIELD: chemistry.

SUBSTANCE: invention relates to chemical industry and can be used for chromatographic separation of fullerenes. The method of making a sorbent for separating fullerenes involves formation of a carbon layer on the surface of thermally activated macroporous silochrome through pyrolysis of propargyl alcohol until attaining concentration of carbon on the surface in the range 4.3 wt % to 8.3 wt %, and removal of by-products using a carrier gas. The process is carried out at temperature ranging from 700°C to 900°C in fluidised bed conditions and the carrier gas used is nitrogen or an inert gas.

EFFECT: invention allows for cutting on time for making carbon-containing silica sorbents, designed for separating fullerenes.

3 cl, 5 ex, 6 tbl, 6 dwg

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RU 2 373 992 C1

Authors

Postnov Viktor Nikolaevich

Blokhin Aleksandr Andreevich

Keskinov Viktor Anatol'Evich

Krokhina Ol'Ga Aleksandrovna

Dates

2009-11-27Published

2008-03-31Filed