FIELD: metallurgy.
SUBSTANCE: procedure consists in settling silver with addition of zinc powder. Before sedimentation of silver zinc powder is preliminary activated in 1-5 % solution of HCl at temperature 80-100°C. Lead chloride at amount of 2-15 g/dm3 is added into chloride solution before sedimentation. The procedure of sedimentation consists in adding activated zinc powder to chloride solution heated to 50-60°C and in successive conditioning for forming a lead sponge and sedimentation of silver on it. After conditioning the formed sponge is broken and solution is mixed. Activated powder of zinc is added in big portions.
EFFECT: raised efficiency of chloride solution purification, increased output of silver, reduced consumption of zinc and time of sedimentation, and thereby reduced cost of process.
2 cl, 1 tbl, 3 ex
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