FIELD: chemistry.
SUBSTANCE: disclosed is a method of producing granular ammonium nitrate which involves neutralisation of nitric acid with gaseous ammonia, evaporation of the obtained solution until obtaining a highly concentrated melt which contains ammonium nitrate in amount of not less than 99.5%, spraying the melt into a granulation tower having at least one vibrogranulator, while feeding air in a counterflow at a rate of 7.0-7.8 t/h per m2 of the cross-section of the tower and output of the obtained granules in amount of 1.0-1.2 t/h per m2 of the cross-section of the tower, cooling the obtained granules with air in fluidised bed apparatus, where after cooling the granules to temperature not over 45°C, spent air at temperature 60 - 70°C comes out of the fluidised bed apparatus into the bottom part of the granulation tower, where it mixes with air sucked from the atmosphere in volume ratio of 1:1, spent air and juice vapour from the neutralisation and evaporation steps are mixed with spent air from the granulation tower, the vapour-air mixture formed is washed in a gas cleaner, while sprinkling the trays of the gas cleaner with a circulating ammonium nitrate solution and further filtered through a multilayer fibrous non-woven material which contains ultrafine fibre, while sprinkling the front layer of the material with condensate of the juice vapour.
EFFECT: invention enables to intensify the process while improving the quality of the end product and reducing harmful emissions into the atmosphere.
3 cl, 1 dwg, 1 ex
| Title | Year | Author | Number | 
|---|---|---|---|
| GRANULATED AMMONIUM NITRATE PRODUCTION PROCESS | 1999 | 
 | RU2147554C1 | 
| PROCESS FOR PREPARING FERTILIZER | 0 | 
 | SU1647001A1 | 
| 0 | 
 | SU470509A1 | |
| METHOD OF PRODUCING AMMONIUM NITRATE AND FILTER ELEMENT FOR FINE PURIFICATION OF GAS-VAPOUR MIXTURE FROM AMMONIUM NITRATE AND AMMONIA BEFORE RELEASE INTO ATMOSPHERE | 2008 | 
 | RU2401247C2 | 
| METHOD FOR PRODUCTION OF AMMONIUM NITRATE | 1990 | 
 | RU2049725C1 | 
| POROUS GRANULATED AMMONIUM NITRATE PRODUCTION PROCESS | 2006 | 
 | RU2311344C1 | 
| METHOD OF PRODUCTION OF POROUS GRANULATED AMMONIUM NITRATE | 2004 | 
 | RU2261226C1 | 
| 0 | 
 | SU117660A1 | |
| METHOD OF PREPARING AMMONIUM NITRATE GRANULES | 2001 | 
 | RU2241691C2 | 
| METHOD FOR PREPARING POROUS GRANULATED AMMONIUM NITRATE | 2004 | 
 | RU2261842C1 | 
Authors
Dates
2011-02-10—Published
2009-08-17—Filed