METHOD OF EXTRACTING BUTADIENE-(ALPHA-METHYL)-STYRENE RUBBER FROM LATEX Russian patent published in 2012 - IPC C08C1/15 C08C1/14 C08F6/14 C08F6/22 C08F236/10 

Abstract RU 2447087 C2

FIELD: chemistry.

SUBSTANCE: invention relates to extraction of synthetic rubber from latex, particularly extraction of butadiene-(alpha-methyl)-styrene rubber. The method of extracting butadiene-(alpha-methyl)-styrene rubber from latex, which is stabilised with carboxylic acid soap and sodium salt of naphthalene sulphonic acid, is carried out using 0.5% sulphuric acid solution and a polyelectrolyte coagulant. The polyelectrolyte coagulant is an epichlorohydrin and dimethylamine copolymer obtained with molar ratio of reactants (1.03-1.10):1, or is a product of reaction of natural and organic compounds, having free amine groups, obtained by grafting a synthetic polymer to a carbohydrate backbone under the effect of an enzyme, said synthetic polymer forming side chains of the polyelectrolyte or poly(N[-3,5-ditertbutyl-4-oxybenzyl)ethylene amine. Latex is introduced into a serum medium which contains sulphuric acid and the polyelectrolyte coagulant at a rate which prevents formation lumps at temperature 20-40°C. Further, the formed rubber crumbs are separated from the serum, washed with water at pH 6.5-8.0 and the rubber crumbs are separated from the washing water, dehydrated, dried and briquetted.

EFFECT: higher extraction of rubber due to considerably low stickiness of the formed rubber crumbs.

1 tbl, 15 ex

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RU 2 447 087 C2

Authors

Golovacheva Ol'Ga Alekseevna

Zotova Natehlla Nikolaevna

Krjuchkova Natal'Ja Valerievna

Orlov Jurij Nikolaevich

Sukhotin Aleksandr Evgen'Evich

Shvareva Galina Nikolaevna

Dates

2012-04-10Published

2010-04-14Filed