FIELD: chemistry.
SUBSTANCE: invention can be applied in production of highly strong complex carbon threads and composition materials for auto- and/or aircraft construction. Carbon-containing component, activator and precursor of catalyst of growing carbon nanopipes are introduced in flow of gas-carrier through device for their introduction with formation of mixture. Obtained mixture is passed through vertical reactor with work chamber, heated to 1000 to 1200 °C by device for its heating. Formed nanopipes are brought out into product receiver. Mixture is supplied into reactor from bottom to top with linear speed from 50 to 130 mm/s. When said work temperature is reached in mixture flow, its linear speed is reduced to 4-10 mm/s, and before output from reactor is increased to 30-130 mm/s. Chamber of reactor is made from three successive sections - lower input 16, middle 17 and upper output 18. Diameter of section 16 constitutes from 1/3 to 1/5 from section 17 diameter, and diameter of section 18 constitutes from 1/3 to 1/4 of section 17 diameter. Output of device for mixture supply into work chamber is connected with input of lower input section 16.
EFFECT: plaints of long multi-layer and well-oriented nanopipes are obtained, stability of continuous process is ensured.
9 cl, 9 dwg, 2 tbl, 40 ex
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Authors
Dates
2013-11-10—Published
2011-11-29—Filed