FIELD: nanotechnology.
SUBSTANCE: invention relates to the technology of production of gold nanoparticles. The method of production of gold nanoparticles from the raw material containing iron and non-ferrous metals comprises preparation of the chlorazotic acid solution of gold using chlorazotic acid. Then floatation extraction of gold precursors is carried out with cationic surfactants from the solution, separation and evaporation of the organic phase to concentrate the gold precursors. Then the concentrate reduction is carried out to obtain dispersion of gold nanoparticles. At that the starting material is first treated with hydrochloric acid to form the insoluble precipitate. Production of chlorazotic acid solution is carried out by dissolving in chlorazotic acid solution of insoluble precipitate. Before floatation extraction of precursors the nitric acid is removed from chlorazotic acid solution with methyl or ethyl alcohol or hydrochloric acid.
EFFECT: improvement of efficiency of the method of production of nanoparticles, namely the increase in the number of gold nanoparticles obtained or its hybrids with noble metals.
3 ex
Title | Year | Author | Number |
---|---|---|---|
PROCEDURE FOR PRODUCTION OF NANO PARTICLES OF GOLD FROM IRON ORE STOCK | 2009 |
|
RU2424339C1 |
METHOD OF AUTOMOTIVE CATALYST | 2011 |
|
RU2464088C1 |
METHOD OF OBTAINING CATALYST ON POROUS METAL OXIDE CARRIER FOR CARBOHYDRATE OXYDATION | 2011 |
|
RU2468861C1 |
METHOD OF PRODUCTION OF PLATINUM METALS NANOPARTICLES | 2006 |
|
RU2333077C1 |
METHOD OF REMOVING PLATINUM METALS FROM MATERIAL CONTAINING THESE METALS | 1997 |
|
RU2120485C1 |
METHOD FOR EXTRACTION OF GOLD FROM AQUA REGIA AND HYDROCHLORIC ACID SOLUTIONS | 1990 |
|
RU1741436C |
METHOD OF RECOVERING PRECIOUS METALS FROM SECONDARY MATERIAL, PREDOMINANTLY FROM TIN-LEAD SOLDER ALLOY | 1996 |
|
RU2099434C1 |
METHOD FOR PRODUCING NANOSCALE TITANIUM DIOXIDE WITH VARIABLE OPTICAL PROPERTIES MODIFIED WITH METALLIC PLASMON NANOPARTICLES | 2021 |
|
RU2771768C1 |
METHOD OF RECOVERING SILVER, GOLD, PLATINUM, AND PALLADIUM FROM SECONDARY MATERIAL CONTAINING PRECIOUS METALS | 1995 |
|
RU2089635C1 |
METHOD OF SEPARATION OF METALLIC PALLADIUM FROM WASTE MANGANI-PALLADIUM CATALYST | 2004 |
|
RU2254387C1 |
Authors
Dates
2014-05-20—Published
2012-03-20—Filed