METHOD FOR CONTINUOUS INDUSTRIAL PRODUCTION OF GLYOXAL Russian patent published in 2016 - IPC C07C45/38 C07C47/127 

Abstract RU 2599247 C1

FIELD: technological processes.

SUBSTANCE: present invention relates to a continuous method of producing glyoxal by oxidation of ethylene glycol with atmospheric oxygen in a mixture with recirculating inert gas on a catalyst containing silver. Recirculating gas used as a diluent and ethylene glycol solution entering reactor are successively pre-heated by heat generated during oxidation of ethylene glycol at catalyst, and cooling of reaction products is performed in successively by their irrigation with cooled solution of glyoxal in a zone lying immediately behind catalyst layer and in tubular sub-contact 2-sectional heat exchanger, in lower section of which ethylene glycol is heated, and in upper section - heating of recirculating gas used as a diluent.

EFFECT: proposed method enables to obtain an end product with high output.

7 cl, 3 dwg, 1 tbl, 3 ex

Similar patents RU2599247C1

Title Year Author Number
METHOD FOR PREPARING GLYOXAL-CONTAINING PRODUCTS 2006
  • Khokhlov Sergej Leont'Evich
  • Petrov Lev Alekseevich
  • Murashova Irina Borisovna
  • Vakhonin Valerij Jur'Evich
RU2321577C2
GLYOXAL PRODUCTION CATALYST 2004
  • Kurina Larisa Nikolaevna
  • Vodjankina Ol'Ga Vladimirovna
  • Knjazev Aleksej Sergeevich
  • Shmotin Viktor Sergeevich
  • Boronin Andrej Ivanovich
RU2278729C1
GLYOXAL PRODUCTION CATALYST 1996
  • Petrov L.A.
  • Rozanov I.G.
  • Kolpakov S.N.
  • Shevchuk S.A.
  • Shamin A.A.
  • Alekhin A.V.
  • Balakin V.M.
RU2119385C1
CATALYST FOR GLYOXAL SYNTHESIS AND METHOD OF GLYOXAL SYNTHESIS 2007
  • Vodjankina Ol'Ga Vladimirovna
  • Knjazev Aleksej Sergeevich
  • Magaev Oleg Valer'Evich
  • Izaak Tat'Jana Ivanovna
RU2340395C1
IMPROVED METHOD OF ETHYLENE OXIDE EXTRACTION 2009
  • Ozero Brajan
RU2525237C2
METHOD FOR PREPARING FORMALIN 2002
  • Kaluzhnikov V.V.
  • Kochergin Aleksandr Nikolaevich
  • Bondar' Petr Fedorovich
  • Kuleshov Nikolaj Pavlovich
RU2233263C2
METHOD OF PRODUCING CARBAMIDE-FORMALDEHYDE CONCENTRATE 2018
  • Afanasev Sergej Vasilevich
  • Volkov Vladimir Anatolevich
RU2685503C1
PROCESS FOR PREPARING METHANIC CHLOROHYDROCARBONS 1996
  • Denisov A.K.
  • Dedov A.S.
  • Golubev A.N.
  • Zakharov V.Ju.
  • Machekhin G.N.
  • Selivanov N.P.
RU2127245C1
TECHNOLOGY OF INDUSTRIAL SYNTHESIS OF GLYOXAL FROM MONOETHYLENE GLYCOL USING INDUSTRIAL SILVER CATALYST DEPOSITED ON ALUMINOSILICATE, CONTAINING 32-36 WT % SILVER 2007
  • Stepanova Lidija Avramovna
  • Armantovich Mikhail Vladimirovich
  • Vanchuk Ehduard Ivanovich
  • Lesogor Tat'Jana Sergeevna
  • Gridin Vladimir Nikolaevich
RU2381210C2
METHOD FOR PRODUCTION AND AUTOMATION OF CONTROL SYSTEM FOR N,N-DIMETHYLACETAMIDE PRODUCTION PROCESSES 2014
  • Luk'Janov Vasilij L'Vovich
  • Dubrovskij Il'Ja Ivanovich
  • Khitrov Nikolaj Vjacheslavovich
  • Glebov Mikhail Borisovich
  • Gordeev Lev Sergeevich
  • Gordeeva Julija L'Vovna
  • Efremov Anatolij Il'Ich
  • Jurasova Galina Stepanovna
RU2568120C1

RU 2 599 247 C1

Authors

Knyazev Andrej Sergeevich

Knyazev Aleksej Sergeevich

Vodyankina Olga Vladimirovna

Dakhnavi Eldar Musaevich

Dates

2016-10-10Published

2015-11-02Filed