FIELD: organic chemistry. SUBSTANCE: product: N-[((2,5-dimethylphenyl)sulfonyl)-aminocarbonyl] -amide of phenoxyacetic acid of the formula C6H5OCH2C(=O)NHC(=O)NHSO2-gu-CH3-2,5, empirical formula is C17H18N2O4S, yield is 89.3% , m. p. is 177-179 C. Reagent 1: phenoxyacetic acid amide. Reagent 2: 2,5-dimethylphenylsulfonylisocyanate. Reaction conditions: anhydrous toluene, at 60-65 C for 10 h. Synthesized compound is used in agriculture. EFFECT: improved method of synthesis, increased yield of product. 2 tbl
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Authors
Dates
1995-03-27—Published
1991-01-14—Filed