METHOD FOR PRODUCING 2-METHYL-6-NITROPHENOL Russian patent published in 1994 - IPC

Abstract RU 2009121 C1

FIELD: organic chemistry. SUBSTANCE: o-cresol is used as reagent 1, sodium nitrite is used as reagent 2. Reaction is carried out in trifluoroacetic acid and glacial acetic acid medium in the presence of acetate of copper monohydrate, molar ratio o-cresol: sodium acetate : acetate of copper monohydrate: trifluoroacetic acid being 1: (1.5-2.5): (0.5-0.6): (4-10.7). The process takes place within 2-2.5 h at 5-10 C, sustaining time being 7-9 h, it is followed by oxidation thus prepared copper complex. Desired product possesses biological activity. EFFECT: improves efficiency of the method.

Similar patents RU2009121C1

Title Year Author Number
METHOD OF 3-NITROSALICYLIC ALDEHYDE SYNTHESIS 1990
  • Shpinel' Ja.I.
  • Mel'Nikov E.B.
  • Beljaev E.Ju.
  • Suboch G.A.
RU2015137C1
0
SU455095A1
METHOD OF PREPARING NITROSOPHENOLS 0
  • Belyaev Evgenij Yurevich
  • Tovbis Mikhail Semenovich
  • Gornostaev Leonid Mikhajlovich
  • Eltsov Andrej Vasilevich
SU726082A1
PROCESS FOR PREPARING NITROSO UREA DERIVATIVES 0
  • Kendzi Tsudzikhara
  • Masakatsu Ozeki
  • Esikhisa Arai
SU908247A3
METHOD OF PRODUCING 2,3,5,6-TETRABROMO-4-NITROPHENOL 2010
  • Vasin Viktor Alekseevich
  • Tarasova Irina Vjacheslavovna
  • Fadin Mikhail Valer'Evich
RU2426723C1
METHOD OF SYNTHESIS OF 2-CHLORO-4-NITROPHENOL 1993
  • Suboch Georgij Anatol'Evich
  • Beljaev Evgenij Jur'Evich
  • Repjakh Stepan Mikhajlovich
RU2046794C1
METHOD AND APPARATUS FOR PRODUCING PARACETAMOL FROM PHENOL 2023
  • Kucherov Fedor Alekseevich
  • Konstantinov Igor Olegovich
  • Rezekin Igor Gennadevich
  • Amochkin Kirill Aleksandrovich
RU2814270C1
METHOD OF PREPARING LYSERGIC ACID AMIDES OR SALTS THEREOF 0
  • Erzhebet Mago
  • Jozhef Borshi
  • Laslo Tardosh
  • Ildiko Kiral
  • Shandor Elek
  • Ishtvan Elekesh
SU604493A3
0
SU427921A1
NITROZO-PYRIDINOL ESTERS DERIVATIVES AS VULCANIZING AGENT FOR CHLOROPRENE RUBBER AND PROCESS FOR PREPARING THEM 0
  • Belyaev Evgenij Yurevich
  • Suboch Georgij Anatolevich
  • Kuznetsova Galina Nikolaevna
  • Semichenko Elena Sergeevna
  • Cherenyuk Ivan Petrovich
SU1047902A1

RU 2 009 121 C1

Authors

Shpinel' Ja.I.

Mel'Nikov E.B.

Beljaev E.Ju.

Dates

1994-03-15Published

1990-04-19Filed