FIELD: chromatography. SUBSTANCE: novel method comprised steps of applying sample including hydantoin, 1-aminohydantoin, furadoin and furagin to thin-layer chromatographic plate, chromatography using admixture of chloroform and methanol as mobile phase, chlorination with use of free chlorine and sprinkling with potassium iodide dissolved in ethyleneglycol. Thus obtained colored product was scraped off into beaker, diluted with water and then treated with N, N-dimethyl-n-phenylenediamine dihydrochloride dissolved in 95-percent solution of ethanol. EFFECT: higher accuracy. 16 tbl
Title | Year | Author | Number |
---|---|---|---|
METHOD OF DETERMINATION OF 5-NITROFURANE DERIVATIVES AND SEMI-PRODUCTS | 0 |
|
SU1748057A1 |
METHOD OF QUANTITATIVE DETERMINATION HYDANTOIN AND ITS DERIVATIVES | 0 |
|
SU1695192A1 |
METHOD OF QUANTITATIVE DETERMINATION OF PHARMACEUTICAL PREPARATIONS BASED ON 5-NITROFURAN DERIVATIVES | 0 |
|
SU1695194A1 |
METHOD OF FURAGIN QUANTITATIVE DETERMINATION | 0 |
|
SU1786405A1 |
METHOD OF QUANTITATIVE DETERMINATION OF FURAGIN | 0 |
|
SU1698716A1 |
METHOD OF QUANTITATIVE DETERMINATION OF FURADONIN | 0 |
|
SU1719972A1 |
METHOD OF NOVOCAINAMIDE ASSAY IN THE OBJECTS OF BIOLOGICAL ORIGIN | 1990 |
|
RU2018113C1 |
Authors
Dates
1994-03-15—Published
1991-10-31—Filed