FIELD: organic chemistry. SUBSTANCE: product: S,S-di-(lower alkyl)-ester of 4-(lower alkyl)-2,6-bis-(trifluoromethyl)-2,6-dihydroxy-3,5-piperidine dicarbothioacid. Reagent 1: lower alkyl thioester of trifluoroacetoacetic acid. Reagent 2: ammonia + lower alkylaldehyde. Reaction conditions: temperature is below 30 C, organic solvent. Synthesized compound is used in agriculture. EFFECT: improved method of synthesis. 2 tbl
| Title |
Year |
Author |
Number |
| METHOD OF SYNTHESIS OF LOWER ALKYL OXY- OR THIO-DERIVATIVES 4-(LOWER ALKYL)-2,6-BIS-(TRIFLUOROMETHYL)-(DIHYDRO- OR TETRAHYDRO)-PYRIDINE-3,5-DICARBOXYLIC ACIDS |
1991 |
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- Khelen Li Janoski[Us]
|
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1991 |
- Vill'Jam Garol'D Miller[Us]
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|
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| METHOD OF OBTAINING DERIVATIVES OF 1,4 OR 3,4-DIHYDROPYRIDINE OR MIXTURE THEREOF |
0 |
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| METHOD OF SYNTHESIS OF DIMETHYL-2-DIFLUOROMETHYL-4-(2-METHYLPROPYL)- 6-TRIFLUOROMETHYL-3,5-PYRIDINEDICARBOTHIOATE |
1991 |
- Khelen Li Dzhanoski[Us]
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1990 |
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| OXAZOLIDINE DIHALOACETAMIDE COMPOUNDS AND A METHOD OF HERBICIDE PHYTOTOXIC EFFECT DECREASE |
1988 |
- Ronald Dzhosef Brinker[Us]
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- Ehrik Li Uilliams[Us]
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| FLUOROALKENYL COMPOUNDS OR THEIR AGRICULTURALLY ACCEPTABLE SALTS FOR STRUGGLE AGAINST PLANT INFECTION WITH NEMATODES, METHOD OF STRUGGLE AGAINST PLANT INFECTION WITH NEMATODES AND METHODS OF SYSTEMIC SUPPRESSION OF PLANT INFECTION WITH NEMATODES |
1992 |
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| METHOD OF SYNTHESIS OF DERIVATIVES OF (S)-3-AMINO-1-BENZYLPYRROLIDINE, DERIVATIVES OF (S)-AZIRIDINE AS INTERMEDIATE COMPOUNDS FOR THEIR SYNTHESIS AND 1-BENZYL-3-(S)-, 2-(S)-[(TERT-BUTOXYCARBONYLAMINO)PROPIONYLAMINO]-PYRROLIDINE AS AN INTERMEDIATE COMPOUND FOR QUINOLONE-BASE ANTIBACTERIAL AGENTS |
1993 |
- Tung Ven Li[Us]
- Gregori Spens[Us]
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1992 |
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RU2102381C1 |
