FIELD: organic chemistry. SUBSTANCE: product: crystalline semihydrate of 4-( 5,6,7,8 -tetrahydroimidazo -[1,5-a]- pyridine -5- yl)- benzonitrile hydrochloride of the general formula. This compound shows a definite interplanar lattice distance (d) and relative line intensity of powder roentgenogram obtained in Guignet's chamber at copper irradiation Kα1, and high stability under condition of relative humidity. Reagent 1: 4-( 5,6,7,8- tetrahydroimidazo- [1,5-a] - pyridine -5- yl)- benzonitrile. Reagent 2: hydrogen chloride. Reaction condition: in the presence of water. EFFECT: improved method of synthesis. 2 tbl
Authors
Dates
1994-10-15—Published
1991-01-11—Filed