FIELD: organic chemistry. SUBSTANCE: product: crystalline 4-(5,6,7,8-tetra- -hydroimidazo-[1,5-a] -pyridine-5-yl)-benzonitrile hydrochloride semihydrate of the formula (I) C14H13N3·HCl·1/2H2O, empirical formula is . Reagent 1: 4-(5,6,7,8-tetrahydroimidazo-[1,5-a]-pyridine-5-yl)- -benzonitrile. Reagent 2: hydrogen chloride. Reaction condition: at 0-70 C. Synthesized compounds were used in medicine, in oncology. EFFECT: improved method of synthesis. 3 tbl
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Dates
1997-08-27—Published
1992-04-07—Filed