METHOD OF SYNTHESIS OF α,5- CYCLO -24R- METHYL -a- CHOLEST -7,22- DIENE-6b-OL Russian patent published in 1994 - IPC

Abstract RU 2024541 C1

FIELD: organic chemistry. SUBSTANCE: product - a,5- cyclo -24R- methyl -a- cholest -7,22- diene -6 b-ol, yield is 94%, m. p. is 95-96 C. Reagent 1: ergosterol. Reagent 2: methanesulfochloride. Reaction conditions: in the medium of pyridine following by treatment with sodium hydrocarbonate in aqueous acetone. Product is used for synthesis phytohormone euibrassinolide. EFFECT: accelerated process, excluding of the end product purification.

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RU 2 024 541 C1

Authors

Khripach Vladimir Aleksandrovich[By]

Zhabinskij Vladimir Nikolaevich[By]

Ol'Khovik Vjacheslav Konstantinovich[By]

Zhernosek Elena Vladimirovna[By]

Dates

1994-12-15Published

1991-06-26Filed