FIELD: organic chemistry. SUBSTANCE: product - bis-(N-nitrosohydroxylamino)-methane disodium salt of the formula NAON(NO)CH2N(NO)ONa, decomposition point is 216 C (explosion). Reagent 1: acetone. Reagent 2: nitrogen oxide. Reaction conditions: in alcohol in the presence of NaOH at the mole ratio reagent 1: reagent 2: NaOH = 4-4.4:1.8-2.0:3. Method is used for synthesis of biologically active substance. EFFECT: improved method of synthesis. 1 tbl
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Authors
Dates
1995-01-27—Published
1990-10-15—Filed