METHOD OF N-BENZOYLCARBAMATE SYNTHESIS Russian patent published in 1995 - IPC

Abstract RU 2033410 C1

FIELD: organic chemistry. SUBSTANCE: reagent 1: benzamide in the form of alkaline-metallic salt where R1 and R2 every means independently halogen. Reagent 2: carbonate of the formula R-O-C(O)OR where C1-C4 - alkyl or phenyl. Reaction conditions: in the medium of organic solvent following by neutralization of prepared product. Preferably to use salt obtained by using lithium, sodium or potassium hydride or hydroxide at temperature from 0 C to boiling point of reaction mixture. Yield of the end product is high, use of toxic benzoylisocyanates is excluded. Synthesized N-benzoylcarbamates show insecticide activity and used for benzoylureas synthesis. EFFECT: high yield of the end product. 3 cl

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RU 2 033 410 C1

Authors

Piter Adrian Verbrjugge[Nl]

Jannete De Val[Nl]

Dates

1995-04-20Published

1990-03-07Filed