FIELD: inorganic chemistry. SUBSTANCE: parental solution containing nickel sulfate is acidified with sulfuric acid up to pH 2.5-6.0, evaporated and the end product is crystallized from evaporated solution by cooling for 2 stages with intermediate exposition at the constant temperature. Solution is cooled at the first stage at the rate 120-720 degree/hr, exposition is performed at 32-35 C for 4-5 hr. EFFECT: improved method of isolation. 1 tbl
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Authors
Dates
1995-12-27—Published
1992-10-09—Filed