METHOD FOR PRODUCTION OF BIS-PHENOLS Russian patent published in 1996 - IPC

Abstract RU 2054411 C1

FIELD: organic chemistry. SUBSTANCE: method involves condensation of pheyl-containing compound with appropriate ketone at their molar ratio (0.81-1.5): 1. The process is carried out in the presence of gaseous HCL as catalyst, said process is followed by blowing reaction mixture with inert gas. Thus obtained product is crystallized in o-xylene, hydrazine or its salt being used as additive (its quantity being 1-15 g per 100 g of origin phenol). Thus prepared crystals are washed by solvent and then are dried at 110-130 C. EFFECT: improves efficiency of method. 1 tbl

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Authors

Khlebnikov B.M.

Valiullina G.A.

Gritsan V.I.

Gritsev V.P.

Panov I.V.

Gritsenko B.D.

Baranov V.P.

Smirnova O.V.

Mikitaev A.K.

Bystrova Eh.I.

Dodonova P.A.

Kotjukova A.L.

Bon A.I.

Zamjatina T.B.

Dates

1996-02-20Published

1993-06-29Filed