FIELD: organic synthesis, more particularly aniline dye industry. SUBSTANCE: product: 7-oxy-5,6- phthalylphenoxazine derivatives of formula I: wherein X is hydrogen, halogen or lower alkyl. Reagent 1: 1- (triazene-N-sulfonate)-2-phenyloxy-4-hydroxyanthraquinone of formula II: . Reaction conditions: in ethylene glycol or glycerol in the presence of alkali at 150-180 C. EFFECT: more efficient preparation process.
Title | Year | Author | Number |
---|---|---|---|
METHOD FOR PRODUCTION OF DERIVATIVES OF 3-PHENYLOXY-5-HYDROXYANTHRA-[1,9-CD]ISOXAZOL-6-ON | 1993 |
|
RU2065438C1 |
METHOD FOR PRODUCTION OF DERIVATIVES OF 7-HYDROXY-5,6-PHTHALYL PHENOXAZINE | 1994 |
|
RU2076103C1 |
METHOD FOR PRODUCTION OF DERIVATIVES OF 3-PHENYLOXY-5-HYDROXYANTHRA-[1,9-CD]ISOXAZOL-6-ON | 1993 |
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METHOD FOR PRODUCTION OF DERIVATIVES OF 5,6-PHTHALYL PHENOTHIAZINE | 1994 |
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RU2072356C1 |
METHOD FOR PRODUCTION OF DERIVATIVES OF 3-PHENYLTHIOANTHRA/1,9-CD/ISOXAZOLE-6-ON | 1994 |
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RU2074183C1 |
METHOD FOR PRODUCTION OF DERIVATIVES OF 5,6-PHTHALYL PHENOTHIAZINE | 1994 |
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RU2076104C1 |
METHOD FOR PRODUCTION OF DERIVATIVES OF 3-PHENYLTHIOANTHRA[1,9-CD]-ISOXAZOL-6-ON | 1994 |
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RU2065440C1 |
METHOD OF PREPARING 7-HYDROXY-5,6-PHTHALYLPHENOXAZINE DERIVATIVES | 0 |
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SU749839A1 |
METHOD FOR PREPARING DERIVATIVES OF 5,6-PHTHALYLPHENOTHIAZINE-S,S-DIOXIDE | 2005 |
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METHOD OF PREPARING SUBERIN FROM BIRCH BARK | 1996 |
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Authors
Dates
1996-09-27—Published
1994-03-05—Filed