FIELD: chemical industry. SUBSTANCE: method involves condensation of carbamide with formaldehyde in alkaline medium in the presence of methanol and esterification of condensation product in acid medium followed by neutralization. Esterification process is carried out by effect on condensation product with aliphatic alcohol taken at 2-4-fold volume with respect to the parent carbamide in the presence of product of alkanols (1-4 carbon atoms) phosphating with phosphoric anhydride. The obtained precondensate has free formaldehyde 0.2 wt. -%, not above, and can be used for carbamide-formaldehyde-base textile material finishing. EFFECT: improved method of preparing. 1 tbl
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Authors
Dates
1997-07-20—Published
1993-07-14—Filed