FIELD: chemical technology, polymers. SUBSTANCE: copolymers of trifluorochloroethylene, alkylvinyl ether and hydroxyalkylvinyl ether were synthesized by copolymerization of the indicated monomers in medium of organic solvent in the presence of radical initiating agent - azocompound and neutralizing agent - ethanolamine of the general formula: (R1)(R2)N - CH2CH2OH where: R1 and R2 - H, -CH3, -C2H5, -CH2CH2OH taken at amount 1-7% of monomers mass. Synthesis is carried out at 55-60 C. At process termination the residual vinyl monomers were distilled off under vacuum. Synthesized copolymers were used for protection of building structures and technological equipment. EFFECT: improved method of synthesis. 2 tbl
Title | Year | Author | Number |
---|---|---|---|
METHOD FOR PREPARING TRIFLUOROCHLOROETHYLENE TERPOLYMER | 2001 |
|
RU2208018C2 |
TRIFLUOROCHLOROETHYLENE TERPOLYMER PRODUCTION PROCESS | 2001 |
|
RU2209215C2 |
METHOD OF PREPARING VINYLIDENE FLUORIDE- TETRAFLUOROETHYLENE COPOLYMERS | 1998 |
|
RU2139891C1 |
METHOD OF SYNTHESIS OF COPOLYMER OF TETRAFLUORO-ETHYLENE WITH PERFLUOROPROPYLVINYL ESTER | 2001 |
|
RU2195465C1 |
PROCESS FOR PRODUCTION TETRAFLUOROETHYLENE COPOLYMERS WITH 2-5 MOL % OF PERFLUOROPROPYL VINYL ETHER | 1999 |
|
RU2156777C1 |
METHOD OF SYNTHESIS OF COPOLYMER OF TETRAFLUORO-ETHYLENE WITH HEXAFLUOROPROPYLENE | 2001 |
|
RU2195466C1 |
COPOLYMERS OF ESTERS OF METACRYLIC ACID AS FILM-FORMING COMPONENTS FOR BINDERS AND COATINGS | 1994 |
|
RU2069667C1 |
MODIFIED TETRAFLUOROETHYLENE/ETHYLENE COPOLYMER PRODUCTION PROCESS | 1999 |
|
RU2156776C1 |
METHOD FOR PREPARING PERFLUORO-2-METHYL-3-OXAHEXANOYLPEROXIDE | 2002 |
|
RU2213730C1 |
METHOD OF SYNTHESIS OF PERFLUORODIACYL PEROXIDE | 2001 |
|
RU2203273C1 |
Authors
Dates
1997-08-27—Published
1994-12-23—Filed