FIELD: chemical industry. SUBSTANCE: preground and diphenyl-amine-free pyroxyline powder is transesterified with acylating mixture of acetic anhydride, methylene chloride and catalyst in 30-60:53-132:0.18-2.0. Pyroxyline powder crumb is first dehydrated with aliphatic alcohol and then extracted with methylene chloride. EFFECT: more efficient preparation method. 2 cl, 1 tbl
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Authors
Dates
1997-10-10—Published
1993-12-20—Filed