FIELD: fine organic synthesis. SUBSTANCE: 2- methyl-2-thiocyanatemethyl-1,3-dioxolane is prepared by reaction of ethylene glycol to form 2,2-dimethyl-1,3- dioxolane which is brominated in CCl4, and the resulting compound is reacted with potassium thiocyanate in DMSO, and reaction mixture in heated to 110-120 C. EFFECT: increased yield of the title compounds and more accessible and cheaper reagents. 2 cl, 2 ex
Title | Year | Author | Number |
---|---|---|---|
N-ISOBUTYL-N-2-TRIMETHYLSILYLOXY(ETHYL)-N-CYCLOHEXANE-2- ONYL(METHYL)AMINE AS INHIBITOR OF CORROSION-MECHANICAL DESTRUCTION OF LOW-ALLOYED STEELS | 1993 |
|
RU2119492C1 |
METHOD OF SYNTHESIS OF 2-(FURYL-2)-1,3-IMIDAZOLIDINES | 1999 |
|
RU2150469C1 |
METHOD OF SYNTHESIS OF 2-(FURYL-2)-1,3-OXAZOLIDINES | 1997 |
|
RU2127272C1 |
METHOD FOR PRODUCTION OF 2-(FURYL-2)-1,3-DIOXANES | 1995 |
|
RU2086550C1 |
COMPOSITE FOR REMOVAL OF PAINT AND VARNISH INSULATING COVER | 2001 |
|
RU2200750C1 |
AGENT "FETIL" FOR PLANT GROWTH REGULATION | 1997 |
|
RU2141202C1 |
METHOD OF PRODUCING ETHYLENE GLYCOL DIACETATE | 0 |
|
SU1698249A1 |
PROCESS FOR PREPARING FILM-FORMING SOLUTION AND PROCESS FOR FORMING DIELECTRIC COATING USING THIS SOLUTION | 1992 |
|
RU2044014C1 |
HERBICIDE | 1994 |
|
RU2127052C1 |
METHOD FOR PRODUCTION OF 2-ALKOXYALKOXIDES OF ALKALINE-EARTH METALS | 1992 |
|
RU2049767C1 |
Authors
Dates
1999-03-27—Published
1997-06-23—Filed