METHOD OF PREPARING 2-METHYL-2-THIOCYANATEMETHYL-1,3- DIOXOLANE Russian patent published in 1999 - IPC

Abstract RU 2128177 C1

FIELD: fine organic synthesis. SUBSTANCE: 2- methyl-2-thiocyanatemethyl-1,3-dioxolane is prepared by reaction of ethylene glycol to form 2,2-dimethyl-1,3- dioxolane which is brominated in CCl4, and the resulting compound is reacted with potassium thiocyanate in DMSO, and reaction mixture in heated to 110-120 C. EFFECT: increased yield of the title compounds and more accessible and cheaper reagents. 2 cl, 2 ex

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RU 2 128 177 C1

Authors

Vershinin S.S.

Makaeva R.M.

Zorin V.V.

Rakhmankulov D.L.

Dates

1999-03-27Published

1997-06-23Filed