FIELD: organic chemistry, more particularly, epoxy resin hardener, initial reactant for synthesis of stabilizers and addition agents to polymeric materials and petroleum products. SUBSTANCE: initial phenol is reacted with aminomethylating agent where aminomethylating agent is mixture of formaldehyde with N,N'-tetramethylmethylene bisamine, and process is carried out in organic solvent at 65-130 C for 30-60 minutes, N,N'-tetramethylmethylene bisamine to formaldehyde molar ratio is 1.00:0.51- 0.55:0.50-0.54, respectively. Organic solvent is preferably aliphatic C1-C4 alcohols in amount of 10-20 wt.%. EFFECT: more efficient preparation method. 3 cl, 14 ex, 1 tbl
| Title | Year | Author | Number |
|---|---|---|---|
| 2,4,6-TRIS(N,N-DIMETHYLAMINOMETHYL)PHENOL PRODUCTION PROCESS | 1998 |
|
RU2146245C1 |
| METHOD OF PREPARING MIXTURE OF PHENOL MANNICH BASES | 1998 |
|
RU2146666C1 |
| BIS-N,N-DIMETHYLAMINOMETHYLATED AROMATIO SCHIFF BASES AND METHOD OF PREPARATION THEREOF | 1998 |
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| N,N-DIMETHYLAMINOMETHYLATED AROMATIC SCHIFF BASES AS HARDENING ACCELERATOR OF EPOXY RESINS, AND METHOD OF PREPARING THEREOF | 1997 |
|
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| METHOD OF PREPARING BIS-N,N(3,5-DI-TERT-BUTYL-4- OXYBENZYL)METHYLAMINE | 1999 |
|
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| METHOD OF PREPARING N,N-DIMETHYL(3,5-DI-TERT-BUTYL-4-HYDROXYBENZYL)AMINE | 2001 |
|
RU2201417C2 |
| METHOD OF PREPARING 2,5-N,N′-(DIMETHYLAMINOMETHYL)-1-4- HYDROQUINONE | 1994 |
|
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| 6,6′-DIMETHYLAMINOMETHYL-1-OXYBENZALDEHYDE AS EPOXY RESIN HARDENER, AND METHOD OF PREPARATION THEREOF | 1995 |
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| METHOD OF PREPARING N,N'-SUBSTITUTED PIPERAZINES | 1998 |
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| PROCESS FOR PREPARING 2-N,N-(DIMETHYLAMINOMETHYL)-PHENOL | 0 |
|
SU1038339A1 |
