FIELD: oil additives. SUBSTANCE: invention, in particular, relates to sulfur- and phosphorus- containing additives possessing elevated antiscoring and antiwear properties as well as high heat and oxidation resistances. Invention provides preparation of dithiophosphate-based lubricant additives for lubrication oils, in particular for reducer oils, consisted in that 8-endooxymethyl-3,4,5-exotrithia-tricyclo[5.2.1.0(2,6)] decan and 2- ethylhexanol or the former compound and isobutyl alcohol are subjected to reaction with phosphorus pentasulfide in mineral oil solution at 80 C followed by treatment of resulting product with zinc oxide at 20 C. EFFECT: provided novel preparation procedure. 1 tbl, 3 ex
Title | Year | Author | Number |
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METHOD FOR PRODUCTION OF O-(2-ETHYL-N-HEXYL)-O-(3,4,5-TRITHIATRICYCLO[5.2.1.0]-DEZ-8-YL-METHYL)-DITHIOPHOSPHORIC 1-(N,N-DIMETHYLAMINOMETHYL)-BENZOTRIAZOLE SALT AS LUBRICANT OIL ADDITION | 2003 |
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METHOD FOR PRODUCTION OF O-(N-BUTYL)-O-(3,4,5-TRITHIATRICYCLO[5.2.1.0]-DEZ-8-YL-METHYL)-DITHIOPHOSPHORIC ACID 1-(N,N-DIMETHYLAMINOMETHYL)-1,2,4-TRIAZOLE SALT AS LUBRICANT OIL ADDITIVE | 2003 |
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METHOD FOR PRODUCTION OF O-(2-ETHYL-N-HEXYL)-O-(3,4,5-TRITHIATRICYCLO[5.2.1.0]-DEZ-8-YL-METHYL)-DITHIOPHOSPHORIC 1-(N,N-DIMETHYLAMINOMETHYL)-1,2,4-TRIAZOLE SALT AS LUBRICANT OIL ADDITIVE | 2003 |
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METHOD FOR PRODUCTION OF O-(n-BUTYL)-O-(3,4,5-TRITHIATRICYCLO(5.2.1.0)DEZ-8-YL-METHYL))-DITHIOPHOSPHORIC ACID 1-(N,N-DIMETHYLAMINOMETHYL)-BENZOTRIAZOL SALT AS LUBRICANT OILINESS ADDEND | 2003 |
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METHOD FOR PRODUCTION OF O-(N-BUTYL)-O-(2-ETHYL-N-HEXYL)-DITHIOPHOSPHORIC ACID 1-(N,N-DIMETHYLAMINOMETHYL)-BENZOTRIAZOLE SALT | 2003 |
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METHOD FOR PRODUCTION OF O-(N-BUTYL)-O-(2-ETHYL-N-HEXYL)-DITHIOPHOSPHORIC ACID 1-(N,N-DIMETHYLAMINOMETHYL)-1,2,4-TRIAZOL SALT | 2003 |
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METHOD OF PREPARING SULFUR-CONTAINING ADDITIVES | 1999 |
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METHOD FOR PREPARING 3-THIA-EXSO-TRICYCLO-[5.2.1.0]-DECANE | 2002 |
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Authors
Dates
2002-09-27—Published
2000-10-30—Filed