FIELD: petroleum processing. SUBSTANCE: composition contains petroleum product and detectable amount of marker, in particular biological pigment preparation "Prodigiosin" in amount (1,2-9,3)•10-6 g/l. Marking is performed by adding to product required amount of marker solution. Identification of petroleum product involves adding developing reagent, in particular 36% aqueous hydrochloric acid solution, which is added in amount 0.33-0,35% to sample depending on the volume of sample. Quantitative content of marker in petroleum product is found by absorption spectrophotometry technique. Marking solution contains marker and solvent, concentration of the former being 0.13-2.20%. Solvent is selected from ethanol, light petroleum, and ethyl acetate. Marker is prepared by growing bacteria Serratia marcescens on agar-supplemented oats medium followed by extraction of 96% ethanol at shaking. Multistep extraction is continued until bacterial mass is decolorized and, after each step, bacterial mass is sedimented and then separated from supernatant. EFFECT: enlarged assortment of markers. 10 cl, 2 tbl, 73 ex
Title | Year | Author | Number |
---|---|---|---|
IDENTIFICATION METHOD OF MARKED OIL PRODUCTS | 2007 |
|
RU2368645C2 |
METHOD OF PRODIGIOSIN PRODUCTION | 2007 |
|
RU2384615C2 |
METHOD OF MANUFACTURING A MARKER OF FUELS AND LUBRICANTS | 2018 |
|
RU2689420C1 |
APPLICATION OF A COMPOSITION INCLUDING MINERAL MOTOR OIL OR INDUSTRIAL OIL, SUSPENSION OF NANOMATERIAL (CNM) AND SURFACE-ACTIVE SUBSTANCE (SAS) FOR OIL PRODUCT MARKING, AND METHOD OF PRODUCT IDENTITY | 2017 |
|
RU2678457C2 |
COMPOSITION INCLUDING PETROLEUM PRODUCT AND THYMOL-PHTHALEINE MARKER, METHOD AND SOLUTION FOR MARKING PETROLEUM PRODUCT, AND A METHOD FOR IDENTIFICATION OF PETROLEUM PRODUCT | 1996 |
|
RU2187539C2 |
COMPOSITION INCLUDING PETROLEUM PRODUCT AND MARKER, METHOD AND MARKING SOLUTION FOR PETROLEUM PRODUCT, AND METHOD FOR IDENTIFYING PETROLEUM PRODUCT | 1996 |
|
RU2159269C2 |
METHOD OF IDENTIFICATION OF PETROLEUM PRODUCT USING MARKER AND DEVELOPING REAGENT | 1996 |
|
RU2187538C2 |
METHOD FOR PRODUCTION OF BACTERIAL PIGMENT PREPARATION | 2004 |
|
RU2283329C2 |
FLUORESCENT LABEL FOR PETROLEUM PRODUCTS | 1995 |
|
RU2149887C1 |
CHEMICAL MARKER AND METHOD FOR PRODUCTION THEREOF | 2011 |
|
RU2489476C2 |
Authors
Dates
2003-12-10—Published
2002-07-22—Filed