FIELD: rubber industry.
SUBSTANCE: curing agent contains, wt %: sulfur 45.0-90.0, 1,4-bis(trichloromethyl)benzene 5.0-40.0, hexamethylenetetramine 1.0-5.0, and wax 2.0-10.0. Agent is prepared by mixing sulfur melt with molten 1,4-bis(trichloromethyl)benzene at 115-120°C followed by adding hexamethylenetetramine and wax, raising temperature to 140-150°C, and stirring resulting melt at this temperature during 30-40 min, whereupon melt is cooled in thin layer to 15-20°C.
EFFECT: improved distribution of curing agent in rubber compound, increased resistance to reversion during prolonged vulcanization of rubber and to thermal-oxidative action.
3 cl, 5 tbl, 7 ex
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Authors
Dates
2005-03-10—Published
2003-02-19—Filed