FIELD: organic chemistry, chemical technology.
SUBSTANCE: invention relates to a method for synthesis of benzofurazans by reduction of benzofuroxanes in ethylene glycol medium. Sulfur is used as a reducing agent and taken in the amount 0.5-1.0 g-atom per 1 g-mole of furoxane, and the process is carried out at temperature 140-155°C. Proposed method for reduction of benzofuroxanes with sulfur in ethylene glycol is safety and economy.
EFFECT: improved method of synthesis.
4 ex
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