FIELD: analytical methods in food industry.
SUBSTANCE: method is characterized by that, when preparing detection device, Al electrodes of 9 piezoelectric resonators of AT cut having intrinsic oscillation frequency 8-10 MHz are modified by applying, using microsyringe, following solutions: polyethylene glycol succinate in ethanolic; polyethylene glycol sebacate, Triton X-100 (ortylpolyethoxyphenol), Tween 40 (polyoxyethylene-sorbitol monopalmitate), and polyethylene glycol adipate in acetone; tetrabenzoate pentaerythritol and polystyrene in chloroform; bis(2-cyanoethyl) ether in toluene; and β-alanine in water so that mass of film on each sensor after removal of solvent in drying box for 30 min at 40°C was 17-25 mkg. Then equilibrium gas phase of curds whey or its fractionation products is sampled and introduced into detection cell. Analytical signals are registered in the form of responses of modified electrodes of piezoelectric resonators every second until equilibrium in sorption system is attained, after which one calculates area of the "visual image" using MS Excell program and plots graduation graph of "visual image" area for curds whey or its fractionation products vs. storage duration. Using this graph, one can calculate storage time for curds whey or its fractionation products.
EFFECT: accelerated analytical procedure and facilitated prediction of storage ability.
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PREDICTING QUALITY OF WHEY AND FRACTIONATION PRODUCT THEREOF | 2008 |
|
RU2383887C1 |
TEST METHOD FOR DETERMINING DEGREE OF OXIDATIVE RANCIDIFICATION OF ANIMAL FAT | 2005 |
|
RU2296323C1 |
METHOD OF FINDING VAPORS OF OIL ACID IN AROMA OF CHEESE SERUM | 2005 |
|
RU2277236C1 |
METHOD OF DETERMINATION OF THE VAPORS OF THE ACETIC ALDEHYDE IN THE AROMA OF THE CURD WHEY | 2006 |
|
RU2315985C1 |
METHOD OF DETECTING LACTIC ACID VAPOUR IN AROMA OF TRUE MILK SOLUTION | 2007 |
|
RU2358263C1 |
METHOD OF ASSESSING ACETIC ACID VAPORS IN WORKING ZONE AIR | 2004 |
|
RU2263908C1 |
METHOD FOR TOTAL DETERMINATION OF C -C -ALKYL ACETATE WORKING ZONE AIR | 2003 |
|
RU2241696C1 |
METHOD FOR RAPID EVALUATION OF SAFETY OF ARTICLES MADE OF PHENOL-FORMALDEHYDE PLASTIC | 2014 |
|
RU2555775C1 |
METHOD FOR TEST-IDENTIFICATION OF MULTI-COMPONENT GASEOUS MIXTURES OF BENZENE, TOLUENE, PHENOL, FORMALDEHYDE, ACETONE AND AMMONIA | 2011 |
|
RU2456590C1 |
METHOD FOR DETERMINING MICRO-CONCENTRATIONS OF ETHYL SPIRITS IN STEAM-GAS MIXTURES | 2007 |
|
RU2321846C1 |
Authors
Dates
2008-01-20—Published
2006-06-20—Filed