DIAMOND-CARBON MATERIAL AND PREPARATION METHOD THEREOF Russian patent published in 2009 - IPC C01B31/06 B01J3/08 B82B3/00 

Abstract RU 2359902 C2

FIELD: chemistry.

SUBSTANCE: invention can be used at production of finishing compositions, film coatings, radiation-resistant materials. The diamond-carbon material contains the carbon in the form of diamond cubic modification and the X-ray amorphous phase in the mass ratio (40-80):(60-20) respectively; the content of said material is as follows (wt %): carbon 89.1-95.2; hydrogen 1.2-5.0; nitrogen 2.1-4.8; oxygen 0.1-4.7; non-combustible admixtures 1.4-4.8. This material is obtained in enclosed volume, in the gas phase inert to carbon by the detonation of carbon-containing explosive with oxygen deficiency placed into the shell of deoxidant-containing condensed phase with deoxidant/carbon-containing explosive mass ratio not less than 0.01:1. The samples of the obtained diamond-carbon material are prepared for elemental analysis by exposition at 120-140°C under vacuum 0.01-10.0 Pa during 3-5 hrs and following treatment at 1050-1200°C by the oxygen flow with the rate providing their combustion during 40-50 s.

EFFECT: invention allows to obtain the product with high carbon content, predictable properties and ultimate composition in the desired phase state.

4 cl, 1 tbl, 25 ex

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RU 2 359 902 C2

Authors

Dolmatov Valerij Jur'Evich

Dates

2009-06-27Published

2005-12-30Filed