METHOD OF OBTAINING 1,3-DIAMINO-5-NITROBENZOLE Russian patent published in 2010 - IPC C07C205/06 C07C209/36 C07C211/49 

Abstract RU 2396245 C1

FIELD: chemistry.

SUBSTANCE: claimed invention relates to improved method of obtaining 1,3-diamino-5-nitrobenzole by reduction of 1,3,5-trinitrobenzole, which is used for synthesis of dyes, medications and polycondensation resins. Method lies in reduction of 1,3,5-trinitrobenzole with hydrogen in methyl alcohol medium in presence of catalytic amounts of palladium catalyst, such as 5% Pd on coal, at temperature 50÷55°C with ratio 6.0-6.05 moles of hydrogen per a mole of 1,3,5-trinitrobenzole.

EFFECT: method allows to increase output of target product, as well as to simplify its separation and reduce process cost.

1 cl, 1 ex

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RU 2 396 245 C1

Authors

Kashaev Viktor Aleksandrovich

Khisamutdinov Gil'Mutdin Khisamutdinovich

Bavrina Alla Pavlovna

Valeshnij Sergej Ivanovich

Il'In Vladimir Petrovich

Sedova Nadezhda Vasil'Evna

Dates

2010-08-10Published

2008-12-29Filed