METHOD OF PRODUCING AROMATIC DIAMINES AND TRIAMINES FROM AROMATIC NITRO-COMPOUNDS Russian patent published in 2015 - IPC C07C209/36 C07C211/55 C07C211/58 C07C211/59 C07C211/56 C07C211/49 C07C211/52 C07D237/36 

Abstract RU 2549618 C1

FIELD: chemistry.

SUBSTANCE: method includes reducing corresponding aromatic di- or trinitro-compounds in the presence of a heterogeneous catalyst in the form of aluminium oxide, using isopropyl alcohol as a solvent. The process is carried out while adding supercritical isopropyl alcohol to a solution of the corresponding di- or trinitro-compound containing isopropyl alcohol, at temperature T=180-360°C and pressure P=150-220 atm. The process is usually carried out in a flow-type tubular reactor.

EFFECT: high efficiency of the process and conducting said process in continuous mode for a few minutes without using expensive catalysts.

2 cl, 6 tbl, 5 ex

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Authors

Sivtsev Vladislav Petrovich

Anikeev Vladimir Il'Ich

Volcho Konstantin Petrovich

Salakhutdinov Nariman Faridovich

Dates

2015-04-27Published

2013-12-18Filed