METHOD OF OBTAINING PECTINE FROM LARCH BARK HAVING MEMBRANE STABILISING ACTIVITY AND CAPACITY TO REDUCE SILVER IONS OF SILVER NANOBIOCOMPOSITE STABILISED WITH PECTINE Russian patent published in 2010 - IPC C08B37/06 B82B1/00 

Abstract RU 2403263 C1

FIELD: chemistry.

SUBSTANCE: invention relates to methods of obtaining pectine polysaccharides from waste wood and can be used in food, pharmaceutical, chemical and other industries. Siberian larch bark (Larix sibirica Ledeb.) and/or Dahurian larch bark (Gmelin) (Larix gmelinii Rupr. (Rupr.)) is prepared for complete extraction of pectine polysaccharides through successive treatment with acetylacetate, water and a solution of oxalic acid.The bark residue is then extracted with an ammonium oxalate solution at 60-70°C for 3-5 hours and then concentrated. The end product is then dropped into 96% ethanol and lyophilically dried.

EFFECT: disclosed method provides high output of up to 12% of pectine polysaccharides from larch bark, having membrane stabilising activity and capable of reducing silver ions from salt solutions to nanosize particles with zero valence, where during the reaction a nanobiocomposite is formed from silver nanoparticles with particle size of 3-27 nm, which are stabilised with an amorphous matrix - pectine.

4 cl, 2 dwg, 1 tbl, 6 ex

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RU 2 403 263 C1

Authors

Babkin Vasilij Anatol'Evich

Ivanova Nadezhda Viktorovna

Trofimova Natal'Ja Nikolaevna

Es'Kova Ljudmila Aleksandrovna

Saljaev Rjurik Konstantinovich

Nurminskij Vadim Nikolaevich

Korzun Aleksandr Mikhajlovich

Feoktistova Ljubov' Prokop'Evna

Sapozhnikov Anatolij Nikolaevich

Likhoshvaj Elena Valentinovna

Arsent'Ev Kirill Jur'Evich

Dates

2010-11-10Published

2009-06-29Filed