FIELD: chemistry.
SUBSTANCE: invention relates to organic chemistry. The described method involves treatment of cyanuric chloride solution in an organic solvent with aqueous sodium azide solution which contains acetic acid. The reaction is carried out at temperature 0-5°C. The solvent used is usually acetone, tetrahydrofuran or acetonitrile. The end product is obtained in a single step without further purification.
EFFECT: improved method for synthesis of 2-azido-4,6-dichlorotriazine (ADCT) which is used in synthesis of the energy-intensive monomer of 2-azido-4,6-bis(propargyloxy)-1,3,5-triazine.
1 cl, 8 ex
| Title |
Year |
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|
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