METHOD OF PRODUCING ACYL FLUORIDE OF PERFLUOROCYCLOHEXANE CARBOXYLIC ACID Russian patent published in 2011 - IPC C07C53/50 C25B3/08 C07C51/00 

Abstract RU 2430909 C1

FIELD: chemistry.

SUBSTANCE: method of producing acyl fluoride perfluorocyclohexane carboxylic acid is realised via electrochemical fluorination of acyl chloride of benzoic acid in liquid anhydrous hydrogen fluoride on nickel anodes in the presence of an electrolyte additive, where the said additive is triallyl amine and the electrolysis process is carried out with pulsed electric current, where electrolysis is carried out in an electrolysis cell with a self-contained separator of the crude material collector.

EFFECT: longer service life of the electrolyte.

2 cl, 1 tbl, 5 ex

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RU 2 430 909 C1

Authors

Kaurova Galina Ivanovna

Lesnevskaja Nina Bolislavovna

Ljudikajnen Aleksandr Aleksandrovich

Matalin Viktor Aleksandrovich

Moldavskij Dmitrij Dmitrievich

Dates

2011-10-10Published

2010-03-17Filed