METHOD OF PRODUCING N-ALKYL-3-METHYL-4-NITROSOANILINES Russian patent published in 2012 - IPC C07C211/52 C07C209/60 

Abstract RU 2470911 C2

FIELD: chemistry.

SUBSTANCE: invention relates to a method of producing novel N-alkyl-3-methyl-4-nitrosoanilines of formula where R=i-Pr, cyclohexyl. The compounds can be used as modifiers and stabilisers of rubber mixtures and as starting compounds for synthesis of N-substituted n-phenylene diamines, which are used to produce a wide range of azo dyes and in colour photography. The method involves cyclocondensation of acetone and the corresponding amine with a product of nitrosation of 4,4-dimethoxybutan-2-one, which is first held in aqueous hydrochloric acid solution.

EFFECT: improved method.

2 ex

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Authors

Suboch Georgij Anatol'Evich

Semichenko Elena Sergeevna

Gavrilova Natal'Ja Alekseevna

Kositsina Anna Sergeevna

Dates

2012-12-27Published

2011-03-29Filed