FIELD: process engineering.
SUBSTANCE: invention relates to production of metal oxide materials, including metal hydroxides and/or metal oxides and catalysts. Proposed method comprises the following steps: dissolving metals in nitric acid to produce metal nitride and releasing NOX and water vapor. Hydrolysis of metal nitride solution by introducing compressed superheated water vapor in metal nitride solution to produce suspension of hydroxide suspension and acid gas. Main components of acid gas are NO2, NO, O2 and water vapor. Suspension filtration and drying to produce metal hydroxides and/or metal oxides. Further recovery of produced metal hydroxides and/or metal oxides and production of metal oxide catalyst in traditional process. Released gas NOX may be used for production of reusable nitric acid. Proposed device consists of system to produce metal salt solution, metal salt solution hydrolysis system, product production system, and system to produce and recycle nitric acid.
EFFECT: continuous production, closed circulation, no emissions, reduced costs.
17 cl, 1 tbl, 2 ex, 1 dwg
Title | Year | Author | Number |
---|---|---|---|
FISCHER-TROPSH SYNTHESIS CATALYST, ITS PRODUCTION AND APPLICATION | 2010 |
|
RU2477654C1 |
METHOD FOR POLYMER CONTAINING SUZUKI REACTION CATALYST PRODUCTION | 2016 |
|
RU2627265C1 |
Fe-BASED CATALYST FOR FISCHER-TROPSCH SYNTGHESIS, METHOD OF ITS MANUFACTURING AND APPLICATION | 2010 |
|
RU2468863C1 |
METHOD FOR PRODUCING A CATALYST FOR THE FISCHER-TROPSCH SYNTHESIS | 2022 |
|
RU2788375C1 |
METHOD OF PROCESSING OF SERPENTINITE | 2005 |
|
RU2292300C1 |
METHOD OF SODIUM NITRITE PRODUCTION | 1993 |
|
RU2069174C1 |
METHOD OF PREPARING SUPPORTED PALLADIUM CATALYSTS | 2004 |
|
RU2282498C2 |
METHOD OF PROCESSING NITRATE SALTS | 2013 |
|
RU2522343C1 |
METHOD FOR OXIDISING AMMONIA AND SYSTEM SUITABLE THEREFOR | 2014 |
|
RU2646643C2 |
PRODUCTION OF RED IRON OXIDE PIGMENT | 2013 |
|
RU2649430C2 |
Authors
Dates
2013-03-20—Published
2009-06-29—Filed